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The desulfurater (BaAl 2 O 4 ) was successfully synthesized with BaCO 3 and Al(OH) 3 powders as raw materials by microwave sintering method. The mass loss of raw materials and the characterization of the outcome were investigated by means of TG-DSC, XRD and optical microscopy. The reaction mechanism was discussed. The experimental results show that synthesized BaAl...