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Polyhydroxyalkanoates (PHAs) showed hierarchical structures and were used as model polymers to investigate the organization process of the high-order structures in biomaterials. Real-time Fourier transform infrared spectroscopy and optical microscopy demonstrated that helical segments formed along with the spherulite growth. Atomic force microscopy revealed the details of growth, twisting and branching...
The isothermal crystallization behaviors of poly(bisphenol A-co-decane ether) (BA-C10) at different temperatures were studied in situ by means of Fourier transform infrared spectroscopic (FT-IR) measurements. Conformational changes during the induction period were investigated in details. The results suggest that conformational changes of polymer chains always take place before the start of changes...
The isothermal crystallization behavior of a poly(bisphenol A-co-decane) (BA-C10) at 35 o C was studied in situ using polarized optical microscopy, atomic force microscopy (AFM) and Fourier transform infrared spectroscopic (FT-IR) measurements. Real-time FT-IR investigation revealed that an increase in regularity as well as intermolecular chain packing of certain functional groups of the BA-C10...
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