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Bilayers of water and p-bromochlorobenzene (BCB) were formed on a surface of Al 2 O 3 (0001) by vacuum deposition under ultra-high vacuum (UHV) conditions with the BCB adlayer on top. The surface was then heated, allowing water that desorbs at a lower temperature to percolate through the upper BCB layer, leading to the formation of clusters. Percolation and cluster formation caused...