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New laser NLO (nonlinear optical) inorganic material nitramino sulphonic acid (NASA) [H 2 N 2 SO 5 ] was synthesized and confirmed by NMR and XRD spectral analysis. NASA crystal was grown from aqueous solution by slow solvent evaporation technique at room temperature. Single crystal XRD revealed that NASA crystallizes in noncentrosymmetric space group P ba2 . The structural...