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A Ni-doped TiO 2 photocatalyst was prepared by polyol method and characterized by ICP-MS, XRD, N 2 adsorption–desorption, SEM, and UV–vis techniques. The effect of preparational parameters such as reduction temperature and reduction time on the degradation of xylene vapor in air under UV light illumination was evaluated. The results revealed that the photocatalytic activity of TiO...