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The synthesis of tailored bioactive carbohydrates usually comprises challenging (de)protection steps, which lowers synthetic yields and increases time demands. We present here a regioselective single‐step introduction of benzylic substituents at 3‐hydroxy groups of β‐d‐galactopyranosyl‐(1→1)‐thio‐β‐d‐galactopyranoside (TDG) employing dibutyltin oxide in good yields. These glycomimetics act as inhibitors...
Fungal β‐N‐acetylhexosaminidases are inducible extracellular enzymes with many biotechnological applications. The enzyme from Penicillium oxalicum has unique enzymatic properties despite its close evolutionary relationship with other fungal hexosaminidases. It has high GalNAcase activity, tolerates substrates with the modified N‐acyl group better and has some other unusual catalytic properties. In...
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