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We have used the techniques of scanning force microscopy (SFM), electron spin resonance (ESR) spectroscopy, ATR IR spectrometry, and powder X-ray diffraction (XRD) to investigate the reaction of methylmethacrylate (MMA) on metal cation-exchanged hectorite thin films. SFM images of the topmost surface of Cu 2+ -, VO 2+ -, and Fe 3+ -exchanged hectorite exposed...