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TiB2/TiC nanocomposite powder was synthesized by ball milling the industrial grade Ti powder and B4C powder. The results show that the milling atmosphere plays a crucial role in the synthesis of TiB2/TiC. After 5 h milling under an appropriate argon protection, a solid state reaction between Ti and B4C occurs resulting in the formation of TiB2/TiC phases. With increasing of the milling time, the crystal...