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The species formed by the anodic oxidation of ethyl xanthate at gold electrodes has been investigated using an ex situ Fourier transform infrared (FTIR) spectroscopic technique to distinguish between chemisorbed ethyl xanthate and diethyl dixanthogen. Chemisorption of xanthate was found to commence about 0.15 V below the potential at which dixanthogen deposits and to reach a fractional surface coverage...