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Elemental powders of Cu (75wt%) and 316-stainless steel (25wt%) has been subjected to ball milling upto 70h followed by isothermal annealing at the temperature range of 350–750°C for 1h to investigate the microstructural evolution along with magnetic and mechanical properties. After 40h of milling, the bcc Fe is almost dissolved in the solid solution of Cu but no significant change has been observed...