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The synthesis and structural study of three new AII(SbV0.5FeIII0.5)(PO4)2 (ABa, Sr, Pb) phosphates belonging to the ASbFePO system were reported here for the first time. Structures of [Ba], [Sr] and [Pb] compounds, obtained by solid state reaction in air atmosphere, were determined at room temperature from X-ray powder diffraction using the Rietveld method. BaII(SbV0.5FeIII0.5)(PO4)2 features the...