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Various aspects of the reactivity of lithium toward propylene carbonate (PC) and poly(ethylene oxide) (PEO) have been examined using ex situ and in situ spectroscopic techniques, respectively. Temperature programmed desorption of perdeuterated PC (d 6 -PC) layers condensed at about 150 K on a clean Li film supported on an Au foil yielded a broad m/e peak, at temperatures in the range from...