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High order aluminosilica monoliths (Al/HOM-5) with cubic Ia3d structures were fabricated with low silica content (Si/Al=1) by means of a simple, reproducible, and one-pot synthesis strategy. A realistic control over the cubic Ia3d geometry of aluminosilica monoliths was achieved by using microemulsion phases of copolymer P123 (EO 20 PO 70 EO 20 ) as soft templates. The textural...