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Several organometallic compounds were examined as second catalyst components (cocatalysts) of the MoOCl 4 -cocatalyst(-EtOH) system with the motivation of development of novel catalysts for the living polymerization of substituted acetylenes. Catalyst systems such as MoOCl 4 -Et 2 Zn-EtOH and MoOCl 4 -n-BuLi have proven to be very effective for the living polymerization...