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The oxidative carbonylation of ethanol to diethyl carbonate (DEC) has been investigated on catalysts prepared by dispersing CuCl 2 and PdCl 2 on activated carbon and carbon nanofibers. The objectives of this work were to establish the effects of support structure and pretreatment on the dispersion of the catalytically active components and, in turn, on the activity and selectivity...
The synthesis of diethyl carbonate (DEC) by the oxidative carbonylation of ethanol was investigated using catalysts prepared by the dispersion of CuCl 2 and PdCl 2 on amorphous carbon promoted with KCl and NaOH. Catalysts were characterized extensively by XRD, XAFS, SEM and TEM with the aim of establishing their composition and structure after preparation, pretreatment, and use. It...
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