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The synthesis of diethyl carbonate (DEC) by the oxidative carbonylation of ethanol was investigated using catalysts prepared by the dispersion of CuCl 2 and PdCl 2 on amorphous carbon promoted with KCl and NaOH. Catalysts were characterized extensively by XRD, XAFS, SEM and TEM with the aim of establishing their composition and structure after preparation, pretreatment, and use. It...