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Bedaquiline is a crucial medicine in the global fight against tuberculosis, yet its high price places it out of reach for many patients. Herein, we describe improvements to the key industrial lithiation‐addition sequence that enable a higher yielding and therefore more economical synthesis of bedaquiline. Prioritization of mechanistic understanding and multi‐lab reproducibility led to optimized reaction...
The effect of support type and alloying with Sn on the electronic structure of supported Pt nanoparticles was investigated using in situ high energy resolution fluorescence-detected X-ray absorption near-edge spectroscopy (HERFD XANES) at the Pt L 3 -edge. Pt and PtSn particles supported on K-L zeolite have similar electronic structures in the presence of individual adsorbates (H 2 ...
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