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The electrolyses of bromoalkyl acrylates were carried out in N,N-dimethylformamide in the presence of a catalytic amount of heptamethyl cobyrinate perchlorate under various reaction conditions. A large-membered cyclic lactone was obtained in a moderate yield. A photo-sensitive intermediate having a cobalt-carbon bond formed during the electrolysis has been characterized using electronic and electrospray...
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