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Using in situ ESR/UV-Vis-NIR cyclovoltammetry at different temperatures, model systems for blue copper proteins like [Cu I (bite)]BF 4 and [Cu II (bite)](BF 4 ) 2 (bite=biphenyldiimino dithioether) were studied with respect to their redox behavior. Chemically reversible processes in the electrode reaction were observed by ESR and UV-Vis-NIR spectroscopy...
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