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The thermal decomposition of ammonium nitrate (AN) laden munitions wastewater and comparable control samples were studied under air and nitrogen environments at pressures from 0.1 MPa to 10 MPa. The decomposition enthalpies, measured using a Differential Scanning Calorimeter (DSC), and gaseous emissions, measured using a Fourier‐Transform Infrared Spectrometer (FTIR), were used to evaluate the quality...