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This article reports the synthesis and tribological behavior of Ti3SiC2‐UHMWPE (Ultra High Molecular Weight Polyethylene) composites for the first time. The compositions were designed by adding 5, 20, and 35 vol% Ti3SiC2 particulates in the UHMWPE matrix. The microstructure evaluation by SEM (Scanning Electron Microscopy) showed that the Ti3SiC2 particles are well dispersed in the green body, but...