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The non‐ionic monomer (methoxy diethylene glycol) acrylate is copolymerized with its azo‐dye‐functionalized acrylate analogue using reversible addition–fragmentation chain transfer (RAFT) polymerization. Copolymerization is increasingly difficult with increasing amounts of the azo‐dye‐bearing monomer. The resulting water‐soluble polymers are thermosensitive, exhibiting lower critical solution temperature...