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A facile inner halogenation of Ag(III) NCP complex 1 is reported. Treatment of 1 with 2N HCl and 1N HBr gave 2 and 4, respectively. A demetallized product 3 was formed as a trace side product when dilute acids were applied and as a predominant product when treated with concentrated acids. The importance of the C3‐ethoxy group for the halogenation reactions was experimentally indicated. Treatment of...