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Two structurally different but chemically similar families of alkyl/siloxane mono‐amidosil hosts, represented by m‐A(x) [where x = 14 or 8 represents the number of CH2 groups of the pendant alkyl chains directly bonded to the carbonyl group of the amide cross‐link] have been doped with a wide range of concentrations of Eu(CF3SO3)3. Mono‐amidosils m‐A(x)nEu(CF3SO3)3 with n ≥ 10 (where n is the molar...