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Single crystals of Tl4.86Fe0.82Hf1.18(MoO4)6 [a = b = 10.5550 (3), c = 37.7824 (9) Å, γ = 120°] are obtained by the self‐flux method in the Tl2MoO4–Fe2(MoO4)3–Hf(MoO4)2 system. On the differential scanning calorimetry curve in the temperature range 320–350 K and at T ∼ 690 K, endothermic peaks are observed. The second harmonic generation test shows an excess of the signal of the quartz standard by...
Microcrystals of MNd(MoO4)2 (M=Rb, Tl) and TlPr(MoO4)2 have been formed with solid state synthesis by the same synthesis route. Final products have been studied by XRD and SEM. Vibrational properties have been evaluated with Raman spectroscopy. More than 20 narrow Raman lines were observed in the experimental spectrum of the microcrystals.
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