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The authors perform a systematic study of the reaction of radical replacement of the dithiocarbonyl group of poly(methyl methacrylate) (PMMA) obtained by reversible addition–fragmentation chain transfer polymerization upon interaction with a radical azo initiator in an inert solvent at 80°C. It is shown that, for a polymer with a dithiobenzoate group, an increase in the molar ratio of the concentrations...