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Samples of Ln2S3 (Ln = Gd, Tb, Dy, Ho, Er, Tm, Yb, and Lu) polymorphs were prepared from Ln2O3 in a CS2 + H2S flow at 1050–1150 °C. DSC melting traces were recorded for Ln2S3 compounds of yttrium lanthanides for the first time. Samples for DSC were prepared by melting and then recrystallizing polycrystalline samples in crucibles of the DSC setup. The melting peak shapes and melting ranges signified...