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Zeolitic imidazolate frameworks (ZIFs) are attractive materials for liquid and gas separations. They are chemically and thermally stable and their pores sizes/pore windows can be modified for enhanced performance. Substituted imidazolate material-1 (SIM-1) is a ZIF that crystallizes in the SOD and RHO topologies. Herein, we report a variety of new syntheses for SIM-1 in the SOD and RHO topologies...