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We have studied the structurally sensitive magnetic susceptibility of intercalates HxNbSe2 (0 ≤ x ≤ 5.2) in the temperature range 4.2 to 300 K (the compound is obtained by intercalation by hydrogen from the gas phase in niobium diselenide powders). We have shown that intercalation leads to a reverse structural transition of the type 2H-TaS2 → 2H-MoS2 at x = 0.92, which is accompanied by an abrupt...