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In the present study, epoxidation and ozonolysis led to a decrease of 40.8 and 51.9 % in the degree of unsaturation of corn oil, respectively. Both products were initially characterized by Fourier transform infrared spectroscopy and 1H- and 13C-nuclear magnetic resonance spectroscopies. The heteronuclear single-quantum correlation spectroscopy (HSQC) analysis of the polyol obtained by epoxidation...