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The formation of the explosive compound NCl 3 during the reaction of ammonium compounds in hydrochloric acid with H 2 O 2 or chlorine as an oxidant was investigated. With the use of H 2 O 2 in the acidity range from 3 to 6 M only traces of NCl 3 were formed. On the other hand, when chlorine was added to 0.01-2 M NH 4 Cl solutions, considerable...
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