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The aim of this study was to investigate interaction between water molecules and internal clay surfaces by means of neutron diffraction and quasielastic neutron scattering. A hydrophobic cation, TMA + (NC 4 H 12 ), was used to saturate the interlayer space of nontronite NAu-1 in order to reduce hydration of interlayer cations that could hinder the effects related to the clay–water...