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Two partially solvated dinuclear complexes of the Ir 24+ core have been prepared from reactions of Ir 2 (COD)(μ-form) 2 (O 2 CCF 3 ) 2 (H 2 O) (1) with an alkylating reagent in acetonitrile. The compound [Ir 2 (COD)(μ-form) 2 (MeCN) 3 ][BF 4 ] 2 (2) is produced in essentially quantitative yields...