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Monodisperse core–shell latices were synthesized, differing in the acrylic acid (AA) content in the particle shell (1 or 4 wt%) and the T g of the acrylic core (around −40 or 10°C). In a first step, the drying mechanisms of the dialyzed latices were studied by confocal Raman spectroscopy. It was shown that, besides some unexpected features (briefly described in the article), drying occurred...