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CuCrTiS 4 was obtained by solid-state synthesis methods. The crystal structure of the quaternary phase was investigated by X-ray powder method and is described in the thiospinel structure (space group Fd¯3m) with the lattice parameter а=0,99388(1) nm. Atomic parameters were refined in the isotropic approximation (R I =0.0465, R P =0.1060). The possibility of the use of this...