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Highly air stable FeCo nanocrystals were synthesized by the proteic sol–gel method using a rotary oven. The synthesized materials were characterized by TG, DTA, XRD, TPR, VSM, Mössbauer spectroscopy and FEG-SEM. The results showed the effect of temperature and the influence of the hydrogen flow rate on the formation of pure FeCo alloy and on the average crystallite size. The use of a rotary oven is...