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Three mononuclear Ni(II), Cu(II) and Zn(II) complexes were prepared by reacting the organic ligand N-phenyl-3-pyridinecarboxamide(NAL) and sodium azide with corresponding metal nitrates in MeOH medium. The isolated metal complexes were characterized by elemental analysis, electronic absorption and infrared spectra. The X-ray crystallographic analysis of the Zn(II) complex revealed a distorted tetrahedral...