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In this Letter, electrohydrodynamic atomisation (EHDA) was used to spray deposit Pt/C catalyst films using a Pt/C nanosuspension. In stable cone-jet atomisation mode, the influence of flow rate on the characteristics of relics and films was analysed. At a lower flow rate smaller size and lower number density of relics were predominant, which led to the formation of porous films; conversely, higher...
A new solid phase microextraction (SPME) method coupled with gas chromatography–mass spectrometry (GC–MS) was developed for rapid determination of four anabolic steroids such as 3α-hydroxy-5α-androstane-17-one (HA), dihydrotestosterone (DHT), androstenedione (AD) and methyltestosterone (MT) in pig urine. SPME was used to extract the four anabolic compounds directly without derivatization. The optimum...
A kind of homemade solid-phase microextraction fibre coupled with gas chromatography–mass spectrometry (GC–MS) was developed for trace analysis of antiestrogens (tamoxifen, cis- and trans-clomiphene) in biological matrices. In this method, derivatization was unnecessary and sample solution could be injected directly after very simple deproteinization operation. The conditions of influencing adsorption...
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