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This is the first evidence for the successful growth of Bi 2 S 3 nanocrystals in glass matrix (SiO 2 –K 2 O–Na 2 O–B 2 O 3 –ZnO–TiO 2 ) using the fusion method. Different sizes of nanocrystals in glass matrix were grown by annealing the glass (dispersed with Bi 2 S 3 nucleons) under two different conditions. The glass...