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The effect of hydroporphine and porphinone macrocycles on the voltammetry and spectroscopy of Fe(P)(NO) was examined. Two oxidation and two reduction waves were observed for all the complexes examined. The variation in the half-wave potentials fell into two categories: those where the E 1 2 of the complex varied linearly with the E 1 2 of the free-based, and those where the relationship was non-linear...