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Radical formation by X-irradiation of single crystals of l-asparagine monohydrate at 275K has been investigated at 240K and 295K using Electron Paramagnetic Resonance (EPR), Electron Nuclear DOuble Resonance (ENDOR) and ENDOR-Induced EPR spectroscopic techniques. Free radical structures suggested by detailed analysis of the experimental data were assessed by Density Functional Theory calculations...