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Porous Ti2O3 was prepared via the carbothermal reduction of titanium dioxide using acetylene black or activated carbon as the reducing agent. The process was carried out at 1300–1350°C in a flowing argon atmosphere or vacuum. The reduced sample had a carbon content of less than 0.007% and a Ti2O3 content of more than 98% when 6.98% acetylene black or 8.88% activated carbon was used as the reducing...
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