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Multi-wall carbon nanotubes (MWCNTs) are filled in the cavity at the tip of a microelectrode to form a carbon nanotube powder microelectrode (CNTPME) for testing the nanotubes under various conditions. Anodic treatment is found to cut the nanotubes into shorter species, increase double layer capacity, and make the nanotubes able to strongly adsorb Os(bpy) 32+ . The CNTPME modified...