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Seven novel Gd(OAc)[S2P(OR)2]2·2CH3CN and Gd(OAc)[S2P(OR′)2]2·2CH3CN gadolinium complexes where R=Et, n-Pr, n-Bu and Ph and R′=CH2CMe2CH2, CH2CEt2CH2, and CMe2CMe2 were synthesized and characterized by elemental analyses, Molecular weight determinations, IR and UV Visible spectroscopy. Micro analytical data revealed a 1:2 metal–ligand (O,O′-dialkyl and alkylene dithiophosphate) molar ratio in all...