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A series of pure solid solution between Li2MO3 and LiNi1/2M1/2O2 (M=Ti, Mn) described as Li5/3Ni1/6Mn5/6-xTixO8/3(0≤x≤5/6) have been successfully prepared. Their hexagonal lattice parameters, a and c, change monotonously with the increase in x value. Tremendous change in their I003/I104 values indicates that Ti substitution causes cation mixing in the solid solution. The shapes in initial charge curve...