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The performance of a second-generation analytical-scale silica monolith utilizing the curtain flow (CF) column design was studied for the first time. The performance of the CF column was compared to a conventional monolith column under isocratic conditions, and the new column achieved a gain in theoretical plates by as much as 50%, with almost Gaussian bands being obtained (asymmetry factor of 1.02)...
“Reaction flow (RF) chromatography” has recently emerged from exploiting a new column “Parallel Segmented Flow” (PSF) to post-column derivatisation (PCD) methods [1]. The main advantage RF has over conventional PCD methods is the elimination of large volume reaction coils, as mixing occurs in the PSF column outlet fitting design, therefore minimising peak broadening. In this investigation we take...
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