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In this paper, polycrystalline bulk Ti 3 SiC 2 samples were synthesized by spark plasma sintering (SPS) of TiC, Ti, Si, and Al powder mixtures. X-ray diffraction (XRD) and scanning electron microscope (SEM) were used for phase identification and microstructure evaluation. The results showed that addition of aluminum can considerably accelerate the synthesis reaction of Ti 3 ...
The dense polycrystalline Ti 2 AlC has been synthesized by spark plasma sintering (SPS) of the elemental Ti, Al and C powders with molar ratio of 2:1.2:1. The bulk material with the high-purity Ti 2 AlC was obtained when treated at 1100 °C, 30 MPa for 1 h. The density was 99.8% of the theoretical value. The obtained Ti 2 AlC had lattice parameters of a=0.3058±0.0002 nm and...
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