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High-temperature Raman scattering measurements of KDP doped with Ni (1% weight) were performed over the spectral range 50–1200cm −1 . The X-ray powder diffraction patterns taken at room temperature and analyzed by Rietveld refinement showed that doped samples of KDP:Ni have the same tetragonal structure of a pure KDP crystal, but with a contraction of the crystalline cell. The behavior of...