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To explore novel nano-scintillator with a controllable architecture, pure and Eu3+ doped lutetium oxyfluoride (Lu7O6F9) powder were synthesized by combining mild hydrothermal method and solid state calcination approach. The products were all pure orthorhombic Vernier phase demonstrated by X-ray powder diffraction (XRD). The detailed crystal structure was also studied by Reitveld refinement. Lath-like...