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This work started with the identification of some operating parameters deviations from the purification module of the Pilot Detritiation Plant, in confront with their design levels, namely: the tritiated heavy water vapor degree of retention in the deuterium flow was more than 5ppm, less than the design value of max. 2ppm; the cooling duration from 128°C to the 20°C was 20h, more than the design value...